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苯乙酮肟的合成

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OCCH31.1 R:H2NOH-HCl, R:K2CO3, rt1.2 1.0 min; cooled(Step 1.2)NOTE: microwave irradiation, Reactants: 1, Reagents: 2, Steps: 1, Stages: 2HON92%PhCMe

Australian Journal of Chemistry, 58(8), 603-606; 2005

OPhCCH3R:H2NOH-HCl, R:NaOH, S:H2O, 3 h, refluxHON88%CMeNOTE: analogs prepared similarly, Reactants: 1, Reagents: 2, Solvents: 1, Steps: 1, Stages: 1

Hunan Shifan Daxue Ziran Kexue Xuebao, 28(1), 56-59; 2005

OPhCCH3R:H2NOH-HCl, R:CaCO3, S:EtOH, 4-6 h, rtHON80%CMeNOTE: Reactants: 1, Reagents: 2, Solvents: 1, Steps: 1, Stages: 1

Zhongguo Yiyao Gongye Zazhi, 35(7), 395-396; 2004

OPhCCH3R:H2NOH-HCl, S:EtOH, S:C5H5N, 2 h, refluxHON91%CMeNOTE: Reactants: 1, Reagents: 1, Solvents: 2, Steps: 1, Stages: 1

Tetrahedron Letters, 46(15), 2599-2602; 2005

OPhCCH3C:Montmorillonite, C:Fe(NO3)3, 95 s, rtHON92%CMeNOTE: microwave irradn., Reactants: 1, Catalysts: 2, Steps: 1, Stages: 1

Oriental Journal of Chemistry, 20(1), 211-212; 2004

CASREACT

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