MS Report from Instrument: LCMS-03 File ..Data\\20170830\\20170830-2\\BIZ2017-830-WYQ5.D Tgt Mass (CHM): Injection Date : 30 Aug 17 2:17 pm +0800 Seq. Line : 12 Sample Name : BIZ2017-830-WYQ5 Location : P1-E-04 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20170830\\20170830-2\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20170830\\20170830-2\\1-POS-3MIN.M Catalog No : HY-101772 Batch#26094 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.2851.3341.4381.4mAU500000.5 DAD1 B, Sig=254,4 Ref=offmAU500000.5 ELS1 A, ELSD SignalmV1005000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70600000040000002000000000.51 Ion 0, MSD1 0,Target Mass 0 Positive, EIC=-0.30:0.700.050-0.05-0.100.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off1.522.5min1.3171.522.5min11.35311.2851.522.5min1.3321.4201.41.4991.6031.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.29 0.02 930.18 927.18 98.39 295 1.33 0.02 13.04 11.34 1.38 5 1.44 0.02 1.17 0.93 0.12 5 1.46 0.02 0.97 0.98 0.10 5 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.29 0.02 1183.22 1184.51 98.08 295 1.33 0.02 21.18 16.05 1.76 5 1.42 0.02 0.44 0.01 0.04 5 1.46 0.01 0.34 0.58 0.03 5 1.50 0.01 0.50 0.06 0.04 615 1.60 0.02 0.73 0.80 0.06 105 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)LCMS-03 8/30/2017 3:08:11 PM SYSTEMPage1 of4MS Report from Instrument: LCMS-03|-------|--------|--------------|--------------|--------|------| 1.32 0.06 22763360.00 6268011.50 100.00 295LCMS-03 8/30/2017 3:08:11 PM SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.32 <<<< POSITIVE SPECTRA >>>> ES-API Positive295.28000006000000100200300400500600700800900m/z591.3611.3200000590.34000005.3LCMS-03 8/30/2017 3:08:11 PM SYSTEMPage3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 8/30/2017 3:08:11 PM SYSTEMPage4 of4
