MS Report from Instrument: HY-LCMS-02 File ..HEM32\\1\\DATA\\20170324\\BIZ\\BIZ2017-324-WJ1.D Tgt Mass (EZX): 274.00 Injection Date : 24 Mar 17 12:29 pm +0800 Seq. Line : 0 Sample Name : BIZ2017-324-WJ1 Location : P1-B-07 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\Chem32\\1\\METHODS\\1-STANDBY.M Catalog No : HY-101426 Batch#24039 Easy-Access Method: '1-POS-3MIN' 274.00 Method Info : Column: A-RP-169 *DAD1 B, Sig=214,4 Ref=off mAU7505001.6081.66625000.5*DAD1 C, Sig=254,4 Ref=off mAU2001.60810000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7010000075000500002500000.511.5 Ion 275, MSD1 275,Target Mass 274 +H Positive, EIC=274.7:275.7 4000030000200001000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.5222.1292.53min1.511.52.2232.12222.1222.53min*22.1272.53min*2.53min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.61 0.02 10.80 8.81 0.85 ND 1.67 0.02 1.45 1.42 0.11 ND 2.12 0.02 1262.43 1094.10 98.98 275 2.22 0.07 0.70 0.81 0.05 275 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.61 0.03 1.00 0.68 0.26 ND 2.12 0.02 375.98 324.49 99.74 275HY-LCMS-02 3/27/2017 9:05:55 AM GZZ_718Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 2.13 <<<< POSITIVE SPECTRA >>>> ES-API Positive1600014000120001000080006000 141.1400020000200300400500600700800900m/z 278.0 277.1 275.0HY-LCMS-02 3/27/2017 9:05:55 AM GZZ_718Page 2 of 2