MS Report from Instrument: HY-LCMS-02 File ..M32\\1\\DATA\\20170308\\CPK\\CPK2017-308-12822.D Tgt Mass (EZX): 461.03 Injection Date : 8 Mar 17 3:01 pm +0800 Seq. Line : 0 Sample Name : CPK2017-308-12822 Location : P1-A-03 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-15832 Batch#12822 Easy-Access Method: '1-POS-3MIN' 461.03 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 C, Sig=254,4 Ref=off 1.6051.2151.3491.4961.5271.6841.74563mAU80060040020000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 708000060000400002000000.511.5 Ion 462.03, MSD1 462.03,Target Mass 461.03 +H Positive, EIC=461.73:462.73 10000800060004000200000.5 Integration Results for DAD1 C, Sig=254,4 Ref=off11.522.5min22.5min1.51.67522.5min* RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.02 1.74 1.78 0.16 ND 1.35 0.02 2.28 1.93 0.22 ND 1.50 0.02 7.67 7.44 0.73 ND 1.53 0.02 4.09 3.72 0.39 ND 1.61 0.02 1034.11 8.42 98.01 461 1.68 0.02 1.72 1.22 0.16 461 1.75 0.01 1.21 1.53 0.11 461 1.75 0.02 2.26 1.84 0.21 461HY-LCMS-02 3/10/2017 2:31:11 PM GZZ_718Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.68 <<<< POSITIVE SPECTRA >>>> ES-API Positive1200010000 463.1 404.1 4.380006000400020000200300400500600700800900m/z 231.9 231.2 461.1HY-LCMS-02 3/10/2017 2:31:11 PM GZZ_718Page 2 of 2
